HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pentyne → HCID 131732124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pentyne | HCID 12309 | — |
| Reactant | But-1-en-1-ol | HCID 143400 | — |
| Reactant | Trimethylsilylmethyl Azide | HCID 150751 | — |
| Reactant | Sodium Ascorbate | HCID 23667548 | — |
| Catalyst | Copper Sulfate | HCID 24462 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131732124 | HCID 131732124 | — |
Reaction Steps
(Azidomethyl)trimethylsilane, pent-1-yne, copper (II) sulfate and sodium (R)-2-((S)-1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydrofuran-3-olate) were added to a 1:2 solution of water:buten-1-ol. The reaction was stirred for about 4 days and t-butanol and water were removed, producing a 4-propyl-1-((trimethylsilyl)methyl)-1H-1,2,3-triazole solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906135B1 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-425e1dd3bb8f4988a61f3e8deb75fb79 |
| Source note | uspto-grants-2014_12 |