HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178456313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-propyl-4-((trimethylsilyl)methyl)-1H-1,2,3-triazole | HCID 131732127 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178456313 | HCID 178456313 | — |
Reaction Steps
1-propyl-4-((trimethylsilyl)methyl)-1H-1,2,3-triazole and excess iodomethane were added to a vial. The reaction was heated for 19.5 hours and 5 mL ACN was added. The reaction was heated for another 2 hours. The precipitate was filtered, rinsed with ether and dried in vacuo overnight. The following 3-methyl-1-propyl-4-((trimethylsilyl)methyl)-1H-1,2,3-triazol-3-ium iodide structure was confirmed:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906135B1 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-d6a1de97a30c4e5790593d24fd7dbf69 |
| Source note | uspto-grants-2014_12 |