Hydrochloric Acid → HCID 70987990, compound

Participants

Reaction Steps

Boc-NH—(CH2)2—N(CH3)—(CH2)5—CONH—(CH2)2-STrt (62.8 mg, 0.11 mmol) was dissolved in THF (6 ml) and HCl in dioxane (130 μl, 4 M solution) was added. The reaction mixture was stirred for 12 h at RT. 200 μl HCl in dioxane was added and the solvent was removed in vacuo. The residue was purified by RP-HPLC to give H2N—(CH2)2—N(CH3)—(CH2)5—CONH—(CH2)2-STrt and not consumed starting material Boc-NH—(CH2)2—N(CH3)—(CH2)5—CONH—(CH2)2-STrt.

Provenance & Evidence