HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 66955493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 2-(4-methyl-6-(4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazin-7-yl)-2-phenylpyrimidin-5-yl)pentanoate | HCID 66956108 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66955493 | HCID 66955493 | 81.2% |
Reaction Steps
This compound was prepared according to general method D from methyl 2-(4-methyl-6-(4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazin-7-yl)-2-phenylpyrimidin-5-yl)pentanoate (0.075 g; 0.174 mmol), sodium hydroxide 10N (0.174 mL; 1.74 mmol) in methanol (1.7 mL) to afford 0.059 g (80%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906906B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-96d78278226945a8b99bcdf6094332cb |
| Source note | uspto-grants-2014_12 |