HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 66955960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 66955574 | HCID 66955574 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66955960 | HCID 66955960 | 13.8% |
Reaction Steps
This compound was prepared according to general method D from methyl 2-(4-methyl-6-(2-oxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)-2-phenylpyrimidin-5-yl)pentanoate (0.180 g; 0.432 mmol), sodium hydroxide 10N (0.432 mL; 4.32 mmol) in methanol (4.3 mL). Purification by preparative HPLC (HPLC method 2) furnished 0.024 g (13%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906906B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-8a3cdbac0d584d47829fbdc42d45a280 |
| Source note | uspto-grants-2014_12 |