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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1399667Generated: November 1, 2026

Sodium Hydroxide → HCID 66955960, compound

https://huagongshe.com/reaction/1399667

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 66955574HCID 66955574—
SolventMethanolHCID 887—
ProductHCID 66955960HCID 6695596013.8%

Reaction Steps

This compound was prepared according to general method D from methyl 2-(4-methyl-6-(2-oxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)-2-phenylpyrimidin-5-yl)pentanoate (0.180 g; 0.432 mmol), sodium hydroxide 10N (0.432 mL; 4.32 mmol) in methanol (4.3 mL). Purification by preparative HPLC (HPLC method 2) furnished 0.024 g (13%) of the title compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08906906B2
Source datasetuspto-grants-2014_12
ORD IDord-8a3cdbac0d584d47829fbdc42d45a280
Source noteuspto-grants-2014_12