HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 50997323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 50997147 | HCID 50997147 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 50997323 | HCID 50997323 | 1.4% |
Reaction Steps
This compound was prepared according to general method D from methyl 2-(4-methyl-6-(3-oxo-2,3-dihydro-1H-inden-5-yl)-2-phenylpyrimidin-5-yl)pentanoate (0.177 g; 0.282 mmol), sodium hydroxide 10N (0.282 mL; 2.82 mmol) in methanol (2.8 mL). Purification by preparative HPLC (HPLC method 1) furnished 0.0016 g (1.4%) of the title compound as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906906B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-62ca598d04c04ce1bb1ed4d00999c0ba |
| Source note | uspto-grants-2014_12 |