Hydrochloric Acid → HCID 71765337, compound

Participants

Reaction Steps

An ice-cold solution of ii (0.25 g, 0.42 mmol) in MeOH-DCM (0.50 and 10 mL respectively) was purged with HCl (g) for 10 min and the mixture stirred at RT for 16 h. The solvent was evaporated and the residue triturated with a mixture of MeOH and Et2O to obtain Compound 2 (0.225 g, 90%).

Provenance & Evidence