HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67980924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67508140 | HCID 67508140 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67980924 | HCID 67980924 | — |
Reaction Steps
To a solution of compound (310 mg, 0.72 mmol) obtained in Step 2, in diethylether (10 mL) was passed HCl gas for about 30 min. at r.t. The solid precipitates were washed with diethylether (10 mL) and ethyl acetate (10 mL) and dried under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906913B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-d508b784162949099383654436e1da1f |
| Source note | uspto-grants-2014_12 |