Hydrochloric Acid → HCID 67443653, compound

Participants

Reaction Steps

To a solution of 132 (272 mg, 0.502 mmol) in DCM (10 mL) was added HCl (4 M in Et2O) (0.502 mg, 2.009 mmol) and the reaction mixture was stirred at RT for 4 hours. The reaction mixture was then concentrated to afford title compound 133 as a yellow solid (244 mg, 100% yield, crude) that was used in the next step with no additional purification. MS (m/z)=486.1 (M+H).

Provenance & Evidence