Hydrochloric Acid → HCID 67410319, compound

HRID 1401256Notes

Reaction equation

HRID 1401256 reaction equation
[OH:1][C:2]1[CH:11]=[C:10]([OH:12])[C:9]([C@@H:13]2[CH2:17][CH2:16][N:15]([CH3:18])[C@H:14]2[CH2:19][OH:20])=[C:8]2[C:3]=1[C:4](=[O:30])[CH:5]=[C:6]([C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([N+:27]([O-:29])=[O:28])[CH:22]=1)[O:7]2.[ClH:31]>CO>[ClH:31].[OH:1][C:2]1[CH:11]=[C:10]([OH:12])[C:9]([C@@H:13]2[CH2:17][CH2:16][N:15]([CH3:18])[C@H:14]2[CH2:19][OH:20])=[C:8]2[C:3]=1[C:4](=[O:30])[CH:5]=[C:6]([C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([N+:27]([O-:29])=[O:28])[CH:22]=1)[O:7]2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67407904HCID 67407904, compound

Product 1

HCID 67410319HCID 67410319, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 25 (0.225 g, 0.545 mmol) was suspended in methanol (2 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-e1a50c52dfcb446d94b2bce36acc7200
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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