Hydrochloric Acid → HCID 67409413, compound

HRID 1401258Notes

Reaction equation

HRID 1401258 reaction equation
[Br:1][C:2]1[C:3]([Cl:29])=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1.Cl>CO>[ClH:29].[Br:1][C:2]1[C:3]([Cl:29])=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67409414HCID 67409414, compound

Product 1

HCID 67409413HCID 67409413, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 29 (0.120 g, 0.24 mmol) was suspended in methanol (2 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-05ffe37bba62424ca3463ab6e2ad7e53
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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