Hydrochloric Acid → HCID 67407911, compound

HRID 1401261Notes

Reaction equation

HRID 1401261 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1.Cl>CO>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 66933697HCID 66933697, compound

Product 1

HCID 67407911HCID 67407911, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 33 (0.140 g, 0.349 mmol) was suspended in methanol (2 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-7c7420cd496e45b1aba1b56761e3cd58
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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