Hydrochloric Acid → HCID 67407638, compound

HRID 1401265Notes

Reaction equation

HRID 1401265 reaction equation
[Cl:1][C:2]1[C:7]([C:8]([F:11])([F:10])[F:9])=[CH:6][CH:5]=[CH:4][C:3]=1[C:12]1[O:13][C:14]2[C:19]([C:20](=[O:22])[CH:21]=1)=[C:18]([OH:23])[CH:17]=[C:16]([OH:24])[C:15]=2[C@@H:25]1[CH2:29][CH2:28][N:27]([CH3:30])[C@H:26]1[CH2:31][OH:32].Cl>CO>[ClH:1].[Cl:1][C:2]1[C:7]([C:8]([F:9])([F:11])[F:10])=[CH:6][CH:5]=[CH:4][C:3]=1[C:12]1[O:13][C:14]2[C:19]([C:20](=[O:22])[CH:21]=1)=[C:18]([OH:23])[CH:17]=[C:16]([OH:24])[C:15]=2[C@@H:25]1[CH2:29][CH2:28][N:27]([CH3:30])[C@H:26]1[CH2:31][OH:32]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67406540HCID 67406540, compound

Product 1

HCID 67407638HCID 67407638, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 41 (0.090 g, 0.192 mmol) was suspended in methanol (1.5 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-b1855f7706204da28621aabe49b16ea2
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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