Hydrochloric Acid → HCID 67408062, compound

HRID 1401267Notes

Reaction equation

HRID 1401267 reaction equation
[Cl:1][C:2]1[C:7]([CH3:8])=[CH:6][CH:5]=[CH:4][C:3]=1[C:9]1[O:10][C:11]2[C:16]([C:17](=[O:19])[CH:18]=1)=[C:15]([OH:20])[CH:14]=[C:13]([OH:21])[C:12]=2[C@@H:22]1[CH2:26][CH2:25][N:24]([CH3:27])[C@H:23]1[CH2:28][OH:29].Cl>CO>[ClH:1].[Cl:1][C:2]1[C:7]([CH3:8])=[CH:6][CH:5]=[CH:4][C:3]=1[C:9]1[O:10][C:11]2[C:16]([C:17](=[O:19])[CH:18]=1)=[C:15]([OH:20])[CH:14]=[C:13]([OH:21])[C:12]=2[C@@H:22]1[CH2:26][CH2:25][N:24]([CH3:27])[C@H:23]1[CH2:28][OH:29]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67407427HCID 67407427, compound

Product 1

HCID 67408062HCID 67408062, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 45 (0.300 g, 0.72 mmol) was suspended in methanol (1.5 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-3fa2b8dd2b5d40a98320b2d35baa1508
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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