Hydrochloric Acid → HCID 67408709, compound

HRID 1401269Notes

Reaction equation

HRID 1401269 reaction equation
[Cl:1][C:2]1[C:7]([N:8]2[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:6][CH:5]=[CH:4][C:3]=1[C:13]1[O:14][C:15]2[C:20]([C:21](=[O:23])[CH:22]=1)=[C:19]([OH:24])[CH:18]=[C:17]([OH:25])[C:16]=2[C@@H:26]1[CH2:30][CH2:29][N:28]([CH3:31])[C@H:27]1[CH2:32][OH:33].Cl>CO>[ClH:1].[Cl:1][C:2]1[C:7]([N:8]2[CH2:9][CH2:10][CH2:11][CH2:12]2)=[CH:6][CH:5]=[CH:4][C:3]=1[C:13]1[O:14][C:15]2[C:20]([C:21](=[O:23])[CH:22]=1)=[C:19]([OH:24])[CH:18]=[C:17]([OH:25])[C:16]=2[C@@H:26]1[CH2:30][CH2:29][N:28]([CH3:31])[C@H:27]1[CH2:32][OH:33]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67408710HCID 67408710, compound

Product 1

HCID 67408709HCID 67408709, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 49 (0.075 g, 0.159 mmol) was suspended in methanol (1 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-a510d33dd71a4167856f741d4a9a8557
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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