Hydrochloric Acid → HCID 67412286, compound

HRID 1401272Notes

Reaction equation

HRID 1401272 reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[C:9]1[O:10][C:11]2[C:16]([C:17](=[O:19])[CH:18]=1)=[C:15]([OH:20])[CH:14]=[C:13]([OH:21])[C:12]=2[C@@H:22]1[CH2:26][CH2:25][N:24]([CH3:27])[C@H:23]1[CH2:28][OH:29].Cl>CO>[ClH:1].[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[C:9]1[O:10][C:11]2[C:16]([C:17](=[O:19])[CH:18]=1)=[C:15]([OH:20])[CH:14]=[C:13]([OH:21])[C:12]=2[C@@H:22]1[CH2:26][CH2:25][N:24]([CH3:27])[C@H:23]1[CH2:28][OH:29]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67409120HCID 67409120, compound

Product 1

HCID 67412286HCID 67412286, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 57 (0.310 g, 0.714 mmol) was suspended in methanol (1.5 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-fb6647229b034a16a810a25f5caf5c58
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

Loading…