Hydrochloric Acid → HCID 67410009, compound

HRID 1401277Notes

Reaction equation

HRID 1401277 reaction equation
[Cl:1][C:2]1[C:7]([NH:8][CH:9]([CH3:11])[CH3:10])=[CH:6][CH:5]=[CH:4][C:3]=1[C:12]1[O:13][C:14]2[C:19]([C:20](=[O:22])[CH:21]=1)=[C:18]([OH:23])[CH:17]=[C:16]([OH:24])[C:15]=2[C@@H:25]1[CH2:29][CH2:28][N:27]([CH3:30])[C@H:26]1[CH2:31][OH:32].Cl>CO>[ClH:1].[Cl:1][C:2]1[C:7]([NH:8][CH:9]([CH3:11])[CH3:10])=[CH:6][CH:5]=[CH:4][C:3]=1[C:12]1[O:13][C:14]2[C:19]([C:20](=[O:22])[CH:21]=1)=[C:18]([OH:23])[CH:17]=[C:16]([OH:24])[C:15]=2[C@@H:25]1[CH2:29][CH2:28][N:27]([CH3:30])[C@H:26]1[CH2:31][OH:32]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67410010HCID 67410010, compound

Product 1

HCID 67410009HCID 67410009, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 65 (0.070 g, 0.153 mmol) was suspended in methanol (1 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-a4402296353e46769f56c8fc180de44c
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

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