Hydrochloric Acid → HCID 67409637, compound

HRID 1401279Notes

Reaction equation

HRID 1401279 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1.[ClH:29]>CO>[ClH:29].[I:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67408796HCID 67408796, compound

Product 1

HCID 67409637HCID 67409637, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of example 69 (0.050 g, 0.101 mmol) was suspended in methanol (1 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title salt.

Workup

  1. customthe organic solvent was evaporated

Sources & evidence

ORD record
ord-54d52da824d2497cbbfae76e965e104c
Source dataset
uspto-grants-2014_12
Patent number
US08906953B2

Reaction notes

Loading…