4-Methoxybenzaldehyde → HCID 89500769, compound

HRID 1401721Notes

Reaction equation

HRID 1401721 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]2[O:8][CH2:9][C:10]([CH2:12][O:13][C:4]=2[CH:3]=1)=[O:11].[CH3:14][O:15][C:16]1[CH:23]=[CH:22][C:19]([CH:20]=O)=[CH:18][CH:17]=1>>[CH3:14][O:15][C:16]1[CH:23]=[CH:22][C:19](/[CH:20]=[C:9]2/[C:10](=[O:11])/[C:12](=[CH:1]/[C:2]3[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=3)/[O:13][C:4]3[CH:3]=[C:2]([CH3:1])[CH:7]=[CH:6][C:5]=3[O:8]/2)=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 312444-MethoxybenzaldehydeHCID 120101Methyl benzodioxepinone

Product 1

HCID 89500769HCID 89500769, compound

Procedure

Calone is reacted with 4-methoxybenzaldehyde analogously to the reaction conditions of Example 1, giving 2,4-bis[1-(4-methoxyphenyl)meth-(Z)-ylidene]-7-methylbenzo[b]-1,4-dioxepin-3-one

Sources & evidence

ORD record
ord-bcedd9d94b724579a4b1416b93c7c6a1
Source dataset
uspto-grants-2014_12
Patent number
US08907110B2

Reaction notes

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