1-Naphthaldehyde → HCID 89500446, compound

HRID 1401729Notes

Reaction equation

[CH3:1][C:2]1[CH:7]=[CH:6][C:5]2[O:8][CH2:9][C:10]([CH2:12][O:13][C:4]=2[CH:3]=1)=[O:11].[C:14]1([CH:24]=O)[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[CH:17]=[CH:16][CH:15]=1>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]2[O:8]/[C:9](=[CH:24]\[C:14]3[C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH:17]=[CH:16][CH:15]=3)/[C:10](=[O:11])/[C:12](=[CH:24]/[C:14]3[C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH:17]=[CH:16][CH:15]=3)/[O:13][C:4]=2[CH:3]=1

Participants

Reactant 2

HCID 61951-Naphthaldehyde

HCID 120101Methyl benzodioxepinone

Product 1

HCID 89500446HCID 89500446, compound

Procedure

Calone is reacted with naphthalene-1-carbaldehyde analogously to the reaction conditions of Example 1, giving 7-methyl-2,4-bis[1-naphthalen-1-yl-meth-(Z)-ylidene]benzo[b]-1,4-dioxepin-3-one.

Sources & evidence

ORD record: ord-782067d00a864cf7b60c914fb60715b1
Source dataset: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08907110B2

Reaction notes

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