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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1401786Generated: October 31, 2026

Aluminium lithium hydride → HCID 67323188, compound

https://huagongshe.com/reaction/1401786

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAluminium lithium hydrideHCID 21226445—
ReactantHCID 67323751HCID 67323751—
SolventTetrahydrofuranHCID 8028—
ProductHCID 67323188HCID 67323188—

Reaction Steps

The preparation was carried out as already described using a 2N lithium aluminium hydride solution in THF starting from 30 mg (0.06 mmol) of ((2S,3S)-3-hydroxypyrrolidin-2-yl)-{4-[4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)thiazol-2-yl]piperidin-1-yl}methanone. The product was purified by means of preparative HPLC and is in the form of the hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08907098B2
Source datasetuspto-grants-2014_12
ORD IDord-3beb4fc1e3434a808a72517ef4ec76b1
Source noteuspto-grants-2014_12