HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxypentanal → HCID 67323291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxypentanal | HCID 20205 | — |
| Reactant | HCID 67325216 | HCID 67325216 | — |
| Product | HCID 67323291 | HCID 67323291 | — |
Reaction Steps
The preparation was carried out as already described via a reductive amination starting from 26 mg (0.05 mmol) of 1-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)isoxazol-5-yl]piperazine and 5 mg (0.05 mmol) of 5-hydroxypentanal. The product was purified by means of preparative HPLC and converted into the hydrochloride by treatment with methanolic HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08907098B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-2b7a054b2b3f4053a1452b12fc2191a3 |
| Source note | uspto-grants-2014_12 |