HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 67324158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 53311875 | HCID 53311875 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67324158 | HCID 67324158 | — |
Reaction Steps
The preparation was carried out as already described starting from 2-[4-(4-hydroxybutyl)piperazin-1-yl]-4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)thiazole-5-carboxylic acid ethyl ester by reduction using a lithium aluminium hydride solution in THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08907098B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-3291e30e70764fd0a47b02d87e07bf86 |
| Source note | uspto-grants-2014_12 |