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HRID1401862

反应详情

EQUATION

反应方程式

HRID 1401862 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC1(C)O[C@H]2[C@H](NC3CCN(c4nc(-c5ccc6c(c5)C(C)(C)CCC6(C)C)cs4)CC3)CCC[C@H]2O1
HCID67323175

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)CCC(C)(C)c2cc(-c3csc(N4CCC(N[C@@H]5CCC[C@@H](O)[C@H]5O)CC4)n3)ccc21
HCID53311876

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

3 ml of 1.25 N HCl in methanol are added to 45 mg of ((3aS,4R,7aR)-2,2-dimethylhexahydrobenzo-1,3-dioxol-4-yl)-{1-[4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)thiazol-2-yl]piperidin-4-yl}amine, and the mixture is stirred at room temperature overnight. The reaction mixture is evaporated and dried under high vacuum. The product is in the form of the hydrochloride.

WORKUP

后处理

  1. customThe reaction mixture is evaporated
  2. customdried under high vacuum