1,2-Dibromoethane → HCID 117734590, compound

Participants

Reaction Steps

0.470 g of ethyl(cyanomethyl)(4-fluorophenyl)phosphinate was initially charged in 20 ml of DMSO, and 0.572 g (4.138 mmol) of potassium carbonate and then 0.388 g of 1,2-dibromoethane were added. The mixture was stirred at room temperature for 4 h and then at 50° C. for 2 h. The reaction mixture was concentrated, taken up in dichloromethane and washed with H2O.

Provenance & Evidence