HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-chlorophenol → HCID 66759860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-chlorophenol | HCID 7265 | — |
| Reactant | 4-(4-Chlorophenyl)dihydro-2H-pyran-2,6(3H)-dione | HCID 104639 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66759860 | HCID 66759860 | 87% |
Reaction Steps
Prepared by dissolving an equimolar mixture of 3-(4-chlorophenyl)glutaric anhydride and commercial 5-chloro-2-hydroxyaniline in boiling dichloromethane. Upon cooling to rt product precipitates and yields after isolation 87% of N-(2-hydroxy-5-chlorophenyl)-3-(4-chlorophenyl)glutaramic acid as colourless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08912186B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-da910cfc6c474ddea5f90e353b664b7c |
| Source note | uspto-grants-2014_12 |