HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-chlorophenol → HCID 66759757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-chlorophenol | HCID 91591 | — |
| Reactant | 4-(4-chlorophenyl)dihydro-2H-pyran-2,6(3H)-dione | HCID 104639 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66759757 | HCID 66759757 | 90% |
Reaction Steps
Prepared by refluxing an equimolar mixture of 3-(4-chlorophenyl)glutaric anhydride and commercial 4-chloro-2-hydroxyaniline in dichloromethane for 0.5 h. After cooling to rt the precipitated product is isolated by suction filtration, washed, and dried to provide 90% of N-(2-hydroxy-4-chlorophenyl)-3-(4-chlorophenyl)glutaramic acid as light red crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08912186B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-48acf899e6bd4bca995364d38e190ca2 |
| Source note | uspto-grants-2014_12 |