Diethyl Malonate → HCID 66759825, compound

HRID 1402856Notes

Reaction equation

HRID 1402856 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:8](=[O:17])[CH:9]=[CH:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:5]=[CH:6][CH:7]=1.[C:18]([O:26][CH2:27][CH3:28])(=[O:25])[CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21]>>[Cl:1][C:2]1[CH:3]=[C:4]([C:8](=[O:17])[CH2:9][CH:10]([CH:19]([C:20]([O:22][CH2:23][CH3:24])=[O:21])[C:18]([O:26][CH2:27][CH3:28])=[O:25])[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=2)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 7761Diethyl MalonateHCID 44219031-(3-chlorophenyl)-3-phenylprop-2-en-1-one

Product 1

HCID 66759825HCID 66759825, compound

Procedure

By a procedure similar to that of example 1.59.2, starting from 1-(3-chlorophenyl)-3-phenylprop-2-en-1-one and diethyl malonate, diethyl 2-[3-(3-chlorophenyl)-3-oxo-1-phenylpropyl]malonate was obtained as colourless solid.

Sources & evidence

ORD record
ord-3bf52b58d16d465aae26c47312221026
Source dataset
uspto-grants-2014_12
Patent number
US08912186B2

Reaction notes

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