Diethyl Malonate → HCID 66759363, compound

HRID 1402866Notes

Reaction equation

HRID 1402866 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13](=[O:22])[CH:14]=[CH:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[CH:7]=[CH:6]2.[C:23]([O:31][CH2:32][CH3:33])(=[O:30])[CH2:24][C:25]([O:27][CH2:28][CH3:29])=[O:26]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13](=[O:22])[CH2:14][CH:15]([CH:24]([C:25]([O:27][CH2:28][CH3:29])=[O:26])[C:23]([O:31][CH2:32][CH3:33])=[O:30])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[CH:7]=[CH:6]2

Participants

3

Reactant 2

HCID 7761Diethyl MalonateHCID 66759472HCID 66759472, compound

Product 1

HCID 66759363HCID 66759363, compound

Procedure

By a procedure similar to that of example 1.59.2, starting from 1-(6-methoxy-2-naphthalenyl)-3-phenylprop-2-en-1-one and diethyl malonate, diethyl 2-[3-(6-methoxy-2-naphthalenyl)-3-oxo-1-phenylpropyl]malonate was obtained as beige coloured solid.

Sources & evidence

ORD record
ord-30cc2963b86c4e80a4fb1da4051ceaa4
Source dataset
uspto-grants-2014_12
Patent number
US08912186B2

Reaction notes

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