2-Acetylnaphthalene → HCID 53676670, compound
Reaction equation
[C:1]([C:4]1[CH:13]=[CH:12][C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=1)(=O)[CH3:2].[Cl:14][C:15]1[CH:22]=[CH:21][C:18]([CH:19]=[O:20])=[CH:17][CH:16]=1>>[Cl:14][C:15]1[CH:22]=[CH:21][C:18]([C:19](=[O:20])[CH:2]=[CH:1][C:4]2[CH:13]=[CH:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[CH:5]=2)=[CH:17][CH:16]=1Participants
3
Procedure
By a procedure similar to that of example 1.59.1, starting from commercial 2-acetylnaphthalene and 4-chlorobenzaldehyde, 1-(4-chlorophenyl)-3-(2-naphthalenyl)prop-2-en-1-one was obtained as yellowish solid.
Sources & evidence
- ORD record
- ord-70c57b4f7460458b8bf2a92e0381a52e
- Source dataset
- uspto-grants-2014_12
- Patent number
- US08912186B2
Reaction notes
Loading…