4-Chlorobenzaldehyde → HCID 66760109, compound

HRID 1402962Notes

Reaction equation

[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.[CH3:10][O:11][CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([C:20](=[O:22])[CH3:21])=[CH:16][CH:15]=1>>[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[CH:21][C:20]([C:17]2[CH:18]=[CH:19][C:14]([O:13][CH2:12][O:11][CH3:10])=[CH:15][CH:16]=2)=[O:22])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 77264-Chlorobenzaldehyde

HCID 44249974'-(METHOXYMETHOXY)ACETOPHENONE

Product 1

HCID 66760109HCID 66760109, compound

Procedure

By a procedure similar to that of example 1.59.1, starting from 4-chlorobenzaldehyde and p-methoxymethoxyacetophenone, 3-(4-chlorophenyl)-1-(4-methoxymethoxy-phenyl)prop-2-en-1-one was obtained as yellowish solid.

Sources & evidence

ORD record: ord-43c269386d45460490e1826cdf575882
Source dataset: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08912186B2

Reaction notes

Loading…