4-Acetylbiphenyl → HCID 53934712, compound

HRID 1402965Notes

Reaction equation

[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.[C:10]1([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:15]=[CH:14][C:13]([C:16](=[O:18])[CH3:17])=[CH:12][CH:11]=1>>[C:10]1([C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH:11]=[CH:12][C:13]([C:16](=[O:18])[CH:17]=[CH:6][C:5]2[CH:8]=[CH:9][C:2]([Cl:1])=[CH:3][CH:4]=2)=[CH:14][CH:15]=1

Participants

Reactant 2

HCID 71134-Acetylbiphenyl

HCID 77264-Chlorobenzaldehyde

Product 1

HCID 53934712HCID 53934712, compound

Procedure

Synthesised according to example 1.59.1 using 4-chlorobenzaldehyde (3.58 g, 25.48 mmol) and 1-(biphenyl-4-yl)ethanone (5.00 g, 25.48 mmol); pale yellow solid; yield: 7.74 g (95%);

Workup

customSynthesised

Sources & evidence

ORD record: ord-090a1afd5aab463588e1d33a28cd77c9
Source dataset: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08912186B2

Reaction notes

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