HRID1403770

反应详情

EQUATION

反应方程式

HRID 1403770 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared according to Procedure A from 4-Chloro-7-iodoquinazoline (0.42 g) and 1-benzyl-1H-indazol-5-ylamine (0.323 g) in acetonitrile (20 ml) at reflux under nitrogen for 18 hours. The mixture was cooled and filtered to give the title compound (0.57 g); m/z (M+1+) 478.

WORKUP

后处理

  1. customPrepared
  2. temperatureat reflux under nitrogen for 18 hours
  3. temperatureThe mixture was cooled
  4. filtrationfiltered