Methanol → HCID 58303961, compound

Participants

Reaction Steps

To a solution of 27-1 (200 mg, 0.57 mmol) in 20 mL of MeOH was added 0.1 g of Pd/C (10%). The mixture was stirred over night under H2 atmosphere at room temperature. The mixture was filtered and the filtrate was to afford 27-2 (150 mg, 0.42 mmol, 74%) as a white solid. LRMS: calc 364.1 and found: 365.1 [MH]+.

Provenance & Evidence