Acetic Anhydride → HCID 58304027, compound

Participants

Reaction Steps

A solution of 30-5 (16 g, 59.7 mmol) in acetic anhydride (50 mL) was stirred at room temperature for one hour. The precipitate was filtered and washed with ether to afford 30-6 (14 g, 76%) as a white solid. LRMS: calc 308.9 and found: 309.9 [M+1].

Provenance & Evidence