Triethylamine → HCID 58303898, compound

Participants

Reaction Steps

A mixture of 30-11 (1.4 g, 4.7 mmol), Pd/C (280 mg, 20%) and Et3N (1.42 g, 14.1 mmol) in MeOH (20 mL) was stirred under hydrogen atmosphere at room temperature overnight. The mixture was filtered and the filtrate was concentrated to afford 30-12 (1 g, 92%) as a yellow solid. LRMS: calc 265.1 and found: 266.1 [M+1].

Provenance & Evidence