HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-bromo-1-ethyl-4-methoxy-1H-indole → 2-(6-bromo-1-ethyl-4-methoxy-1H-indol-3-yl)-N,N-dimethyl-2-oxoacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-bromo-1-ethyl-4-methoxy-1H-indole | HCID 58303909 | — |
| Reactant | 2-(4-Benzyloxy-5-fluoro-1H-indol-3-yl)-N,N-dimethyl-2-oxoacetamide | HCID 66927179 | — |
| Product | 2-(6-bromo-1-ethyl-4-methoxy-1H-indol-3-yl)-N,N-dimethyl-2-oxoacetamide | HCID 58303986 | 88% |
Reaction Steps
Following the procedure (step 5, scheme 1) used to prepare compound 1-6a, compound 36-2 gave compound 36-3 (669 mg, 88%) as a pale pink solid. LCMS: calc 352.0 and found: 353.0 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08912220B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-28c5eae5db254bf6b3a2f6169226b76b |
| Source note | uspto-grants-2014_12 |