反应详情

温度

82 °C

To 3-iodo-2-methoxy-benzoic acid (8.29 g, 29.8 mmol) was added thionyl chloride (15 mL). The resulting solution was stirred for 2 minutes then heated to 82° C. and stirred at this temperature for 30 minutes. The solution was then concentrated under reduced pressure to give the title compound. This material was used without further purification.

1. stirringstirred at this temperature for 30 minutes
2. concentrationThe solution was then concentrated under reduced pressure