HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1404368Generated: November 1, 2026
Thionyl Chloride → 3-Iodo-2-methoxy-benzoyl chloride
https://huagongshe.com/reaction/1404368
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Iodo-2-methoxybenzoic acid | HCID 12168432 | — |
| Product | 3-Iodo-2-methoxy-benzoyl chloride | HCID 86722972 | — |
Reaction Steps
To 3-iodo-2-methoxy-benzoic acid (8.29 g, 29.8 mmol) was added thionyl chloride (15 mL). The resulting solution was stirred for 2 minutes then heated to 82° C. and stirred at this temperature for 30 minutes. The solution was then concentrated under reduced pressure to give the title compound. This material was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08912169B2 |
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| Source dataset | uspto-grants-2014_12 |
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| ORD ID | ord-a0dfb4ece7c749ea94dcf912cc5a2e6c |
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| Source note | uspto-grants-2014_12 |
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