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HRID1404383

反应详情

EQUATION

反应方程式

HRID 1404383 的结构方程式

REACTANTS

反应物

2
反应SMILES：Cl
HCID313

Hydrochloric Acid

ClH

反应SMILES：C[C@@H](CNCCN[C@H]1CC[C@H](CC(=O)N[C@H]2Cc3cccc(C(=O)O)c3OB2O)CC1)NC(=O)OC(C)(C)C
HCID178461770

未命名化合物

PRODUCTS

产物

1
反应SMILES：C[C@H](N)CNCCN[C@H]1CC[C@H](CC(=O)N[C@H]2Cc3cccc(C(=O)O)c3OB2O)CC1
HCID178462034

未命名化合物

PROCEDURE

实验过程

To the compound from step 1 was added 3N HCl (2 ml) and the resultant reaction mixture was heated at reflux for 1 hr. The solvents were then removed in vacuo and the residue purified by reverse phase preparative HPLC and dried using lyophilization. ESI-MS m/z 447 (MH)+.

WORKUP

后处理

  1. customthe resultant reaction mixture
  2. temperaturewas heated
  3. temperatureat reflux for 1 hr
  4. customThe solvents were then removed in vacuo
  5. customthe residue purified by reverse phase preparative HPLC
  6. customdried