HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Dibutylamino)ethanol → N,N-Dibutyl-N-(2-hydroxyethyl)butan-1-aminium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Dibutylamino)ethanol | HCID 7621 | — |
| Reactant | Butyl Chloride | HCID 8005 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N,N-Dibutyl-N-(2-hydroxyethyl)butan-1-aminium chloride | HCID 71334730 | 100% |
Reaction Steps
70 mmol of 2-(dibutylamino) ethanol, 75 mmol of 1-chlorobutane, and 50 g of ethanol were mixed under N2 atmosphere, and made to react at 80 degrees C. for 8 hours under reflux condition. The ethanol and extra 1-chlorobutane were distilled away therefrom by reducing pressure to produce 70 mmol of (2-hydroxyethyl)tributylammonium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08913931B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-4c9a2167d0b84e86a953d28febca755f |
| Source note | uspto-grants-2014_12 |