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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1404928Generated: October 31, 2026

2-(2-Benzothiazolylthio)acetic acid → 2-(Benzothiazol-2-ylsulfanyl)-1-(2-methyl-3,4-dihydro-2H-quinolin-1-yl)-ethanone

https://huagongshe.com/reaction/1404928

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(2-Benzothiazolylthio)acetic acidHCID 80525—
Reactant2-Methyl-1,2,3,4-tetrahydroquinolineHCID 96289—
Product2-(Benzothiazol-2-ylsulfanyl)-1-(2-methyl-3,4-dihydro-2H-quinolin-1-yl)-ethanoneHCID 5946789540%

Reaction Steps

The title compound was synthesized according to General Procedure B using 2-(benzo[d]thiazol-2-ylthio)acetic acid and 2-methyl-1,2,3,4-tetrahydroquinoline to yield 40 as a pale yellow solid (0.32 g, 40%); MS m/z: 355 (M+H)+. Anal. Calcd. For, C19H18N2OS2: C, 64.38; H, 5.12; N, 7.90; S, 18.09. Found: C, 64.38; H, 5.22; N, 7.85; S, 17.93.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08916550B2
Source datasetuspto-grants-2014_12
ORD IDord-f2a59f40cb4b43358b29769dfd97ec07
Source noteuspto-grants-2014_12