HCID 67959218, compound → HCID 67959171, compound

Participants

Reaction Steps

A mixture of tert-butyl 8-[1-(trifluoromethyl)vinyl]-2,3-dihydrothieno[2,3-f][1,4]oxazepine-4(5H)-carboxylate (140 mg), 10% palladium on carbon (50 mg) and ethanol (10 ml) was stirred for 12 hr under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (140 mg, 99.3%) as an oil.

Provenance & Evidence