HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 55080241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-4-chloro-6-methylpyrimidine | HCID 21810 | — |
| Reactant | HCID 86659252 | HCID 86659252 | — |
| Product | HCID 55080241 | HCID 55080241 | — |
Reaction Steps
The title compound is synthesized according to general procedure GP4 (A) starting from 1.5 g (10 mmol) 2-amino-4-chloro-6-methylpyrimidine and 2.7 g (14 mmol) 4-sulfonyl-phenyl boronic acid. After treatment of the precipitated product with diethyl ether 2.3 g (75%) of the desired product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916548B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-c0ae01f4fb8a43138e5f51c3fae28570 |
| Source note | uspto-grants-2014_12 |