Potassium Carbonate → HCID 58513513, compound

Participants

Reaction Conditions

Reaction Steps

The title compound is synthesized according to general procedure GP3 starting from 2.7 g (6.0 mmol) 4-(4-methanesulfonyl-phenyl)-6-methyl-5-trimethylsilanylethynyl-pyrimidin-2-ylamine (A-36) and 415 mg (3.0 mmol) potassium carbonate in 40 mL MeOH. After stirring for 2 h at 0° C. the precipitated product is filtered off and dried over night at 40° C. The product is treated with water, filtered off and dried again. Yield: 1.8 g (83%).

Provenance & Evidence