HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-chloro-4-nitrobenzene → 3-(2-Chloro-4-nitrophenyl)-4-methylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-chloro-4-nitrobenzene | HCID 34667 | — |
| Reactant | 4-Methylpyridine-3-Boronic Acid | HCID 2762711 | — |
| Reactant | 4-(4-methylpyridin-3-yl)-1H-indazole | HCID 66715654 | — |
| Product | 3-(2-Chloro-4-nitrophenyl)-4-methylpyridine | HCID 66714885 | — |
Reaction Steps
Intermediate 27A was prepared from Intermediate 1A and 1-bromo-2-chloro-4-nitrobenzene by the procedure described for the preparation of Intermediate 1C. HPLC Ret timej:1.30 min. MS (ES): m/z=249.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916553B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-6518bae7122f403b901af7aab073f2e3 |
| Source note | uspto-grants-2014_12 |