huagongshe.com
HRID1405173

反应详情

EQUATION

反应方程式

HRID 1405173 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1ccc(F)cc1OCc1ccccc1
HCID2782665

2-Benzyloxy-4-fluorophenylboronic acid

C13H12BFO3

结构：CS(=O)(=O)Cc1cccc(Nc2ncnc(Cl)n2)c1
HCID21956343

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)Cc1cccc(Nc2ncnc(-c3ccc(F)cc3OCc3ccccc3)n2)c1
HCID66571226

未命名化合物

PROCEDURE

实验过程

Example 4 was prepared under similar conditions as described in the preparation of Example 1 using crude 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine and [2-(benzyloxy)-4-fluorophenyl]boronic acid (ABCR GmbH & CO. KG). The batch was purified by preparative HPLC:

WORKUP

后处理

  1. customExample 4 was prepared under similar conditions
  2. customThe batch was purified by preparative HPLC