huagongshe.com
HRID1405174

反应详情

EQUATION

反应方程式

HRID 1405174 的结构方程式

REACTANTS

反应物

2
结构：CC(C)Oc1cc(F)ccc1B(O)O
HCID16217202

{4-Fluoro-2-[(propan-2-yl)oxy]phenyl}boronic acid

C9H12BFO3

结构：CS(=O)(=O)Cc1cccc(Nc2ncnc(Cl)n2)c1
HCID21956343

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)Oc1cc(F)ccc1-c1ncnc(Nc2cccc(CS(C)(=O)=O)c2)n1
HCID66576280

未命名化合物

PROCEDURE

实验过程

Example 5 was prepared under similar conditions as described in the preparation of Example 1 using crude 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine and [4-fluoro-2-(propan-2-yloxy)phenyl]boronic acid (Aldrich Chemical Company Inc.). The batch was purified by preparative HPLC.

WORKUP

后处理

  1. customExample 5 was prepared under similar conditions
  2. customThe batch was purified by preparative HPLC