HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70976411, compound → HCID 89155153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70976411 | HCID 70976411 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89155153 | HCID 89155153 | 93.9% |
Reaction Steps
A solution of 1-chloro-3-[(methylsulfonyl)methyl]-5-nitrobenzene (4.6 g) in methanol (40 mL) was treated similarly as described in example 35.3. Crystallization of the crude product (4.6 g) from diethyl ether furnished the pure title compound (3.8 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916557B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-1337164f9662418ca29df3494d35fa22 |
| Source note | uspto-grants-2014_12 |