Urea → HCID 86723053, compound

HRID 1405615Notes

Reaction equation

HRID 1405615 reaction equation
[CH3:1][N:2]1[C:7]2[CH:8]=[CH:9][CH:10]=[C:11]([CH3:12])[C:6]=2[C:5](=[O:13])[O:4][C:3]1=O.[NH2:15]C(N)=O>>[CH3:1][N:2]1[C:7]2[C:6](=[C:11]([CH3:12])[CH:10]=[CH:9][CH:8]=2)[C:5](=[O:13])[NH:15][C:3]1=[O:4]

Participants

3

Reactant 2

HCID 1176UreaHCID 86723054HCID 86723054, compound

Product 1

HCID 86723053HCID 86723053, compound

Procedure

Starting from 1,5-dimethyl-2H-3,1-benzoxazine-2,4(1H)-dione (prepared according to WO 98/42688) and urea and using Procedure R, the title compound was obtained as an off-white solid (681 mg, 57% yield).

Sources & evidence

ORD record
ord-c64270f661de490c8894ae46599a7ff2
Source dataset
uspto-grants-2014_12
Patent number
US08916573B2

Reaction notes

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